Synthesis of 3-(Tetrahydro-2-furanyl)-5-fluorouracil

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Metabolic activation of R,S-1-(tetrahydro-2-furanyl)-5-fluorouracil (ftorafur) to 5-fluorouracil by soluble enzymes.

There are two major R,S-1-(tetrahydro-2-furanyl)-5-fluorouracil (ftorafur) activation pathways to 5-fluorouracil, one that is mediated by microsomal cytochrome P-450 oxidation at C-5' of the tetrahydrofuran moiety and one that is mediated by soluble enzymes. This report demonstrates that the soluble enzyme pathway proceeds via enzymatic cleavage (possibly hydrolytic) of the N-1--C-2' bond to yi...

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Disposition and Metabolism of 1-(Tetrahydro-2-furanyl)-5-fluorouracil (Ftorafur) in Humans1

The pharmacology of high-dose 1-(tetrahydro-2-furanyl)5-fluorouracil (FT) has been studied by radiochemical and Chromatographie techniques in eight patients. Plasma disappearance of FT was exponential, with a half-life of 8.8 hr. Plasma concentrations of 5-fluorouracil (FUra) were sustained at 12.8 nmol/ml (1.7 /¿g/ml) for at least 48 hr after FT administration. The concentrations of FUra deri...

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5-Fluorouracil concentrations in human plasma following R,S-1-(tetrahydro-2-furanyl)-5-fluorouracil (ftorafur) administration.

Following administration of i.v. doses of fl,S-1 -(tetrahydro-2furanyl)-5-fluorouracil in cancer patients, discrepant results have been obtained by several investigators when assaying for 5-fluorouracil (FUra) plasma concentrations, ranging from 0.1 to 5 fig/ml at peak concentrations. The newly isolated fl,S-1(tetrahydro-2-furanyl)-5-fluorouracil metabolites with altered tetrahydrofuran moiety ...

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Disposition and metabolism of 1-(tetrahydro-2-furanyl)-5-fluorouracil (ftorafur) in humans.

The pharmacology of high-dose 1-(tetrahydro-2-furanyl)-5-fluorouracil (FT) has been studied by radiochemical and chromatographic techniques in eight patients. Plasma disappearance of FT was exponential, with a half-life of 8.8 hr. Plasma concentrations of 5-fluorouracil (FUra) were sustained at 12.8 nmol/ml (1.7 microgram/ml) for at least 48 hr after FT administration. The concentrations of FUr...

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SYNTHESIS AND PHARMACOLOGICAL EVALUATION OF 6-CARBETHOXY-5-(3'-BROMOPHENYL)-3-ARYL-2-CYCLOHEXENONES AND 6-ARYL-4-(3'-BROMOPHENYL)-3-OXO-2,3A,4,5-TETRAHYDRO-2H-INDAZOLES

6-Carbethoxy-5-(3'-bromophenyl)-3-aryl-2-cyclohexenones 2a-j were obtained from the1-Aryl-3-(3'-bromophenyl)-2-propene-1-ones 1a-j by Micheal addition of ethyl acetoacetate, followed by internal Claisen condensation. Reaction of 2a-j with hydrazine hydrate afforded the corresponding 6-Aryl-4-(3'-bromophenyl)-3-oxo-2,3a,4,5-tetrahydro-2H-indazoles 3a-j. The structures of newly synthesized compou...

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ژورنال

عنوان ژورنال: YAKUGAKU ZASSHI

سال: 1978

ISSN: 0031-6903,1347-5231

DOI: 10.1248/yakushi1947.98.11_1551